NMR service can not be considered as responsible in case of loss or diffusion of data that have not been correctly removed from the spectrometer by external/guests users. We therefore ask GUESTS users to directly retrieve their data after acquisition and to erase them from the spectrometer (see 2.2.2).ĭedicated folders are specifically not backed-up. It is also possible to connect directly to the server using the drive mapping process, see below.įor confidentiality reasons, we do not store nor backup any external user data. You can therefore drag them in your computer (left window, blue). In the right window (red one, server) choose the spectro link, then choose the correct spectrometer. Then connect with the following information: This will avoid any modification of the files during the file transfer. In the upper window (Default Transfer Type) choose the "Binary" option. Good sensitivity in 13C and 31P.ĭedicated to short terms experiments FileTypes options. Yes (prodigy, N 2) factor 2 in sensitivityĪUTOMAT,very good sensitivity in 1H and 19F. Good routine machine for 1H, 13C, 19F and 31P.ĪUTOMAT, high sensitivity in 1H, 19F, 13C and 31P, good for characterization. !! GOOD for 1H (zg and COSY) and all reverse experimet Special machine for high pressure measurments
Good routine machine for 1H, 13C, 19F and 31P !! IDEAL for low concentrated 13C samples !! IDEAL for 1H (zg and COSY) and all reverse experiments such HSQC and HMQC. Short to medium experiments for NMR routine 13C samples - Prefer CryoProbes in this caseġH,, very good sensitivity on proton, simple gradient, medium sensitivity on broad band. !! T° limit 0☌ to 60☌ (due to the cryoprobe)ġH, 13C, BB, good sensitivity on carbon and other low gamma nuclei such as 31Pġ5 N, 51 V, 11B are accessible on this machine
Liquid: High resolution, low concentration samples (bio) !! T° limit 0☌ to 80☌ (due to the cryoprobe)
Table of Signal to Noise ratio © Martial Rey Table of all available probes and machines at epfl © Martial Rey
Mestrenova peaks go beneath baseline manual#
Routine TOPSPIN commands for manual machine Available NMR spectrometers and ideal useĤ. If you need some complement, do not hesitate to contact us at pascal.mieville"at"epfl.ch.ġ. We hope you will find here answers to your questions regarding the NMR service of the Institut des Sciences et Ingénieurie Chimiques de l'EPFL.
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